Equipment Chemo-catalytic Conversion

We have comprehensive equipment for the preparation of catalysts and their characterization by different techniques. Further on, we have plenty of different reactor systems which can be used for batch or continuous-flow processes.

Catalyst Preparation

Glass and stainless steel reactors for deposition-precipitation and wet impregnation catalysts
JetCutter and dripping devices for the production of bead-shaped metal oxides by the sol-gel method
Calcination furnaces up to 1200 °C for the treatment of support materials
Reduction furnaces up to 1200 °C for the reduction of catalyst precursors under hydrogen atmosphere

Gallery Catalyst Preparation

Glass reactor (up to 50 g) for preparation of deposition-precipitation and wet impregnation catalysts

Stainless steel reactor (up to 250 g) for preparation of deposition-precipitation and wet impregnation catalysts

Glass reactor (up to 500 g) for preparation of deposition-precipitation and wet impregnation catalysts

JetCutter for bead-shaped support material (Ø = 0.2 – 1 mm)

0.25 mm Al2O3 beads (sol-gel method, JetCutter)

Electrostatic dripping for bead-shaped support materials (Ø > 1 mm)

1 mm Al2O3 beads (sol-gel method, dripping method)

In-situ catalyst activation in fixed-bed reactor

Tube furnace (small) for catalyst activation

Annealing furnace (small) for calcination purposes

Catalyst characterisation

Texture analysis by N₂-adsorption (BET surface area, pore volume, pore size distribution)
ICP-OES for elemental analysis
Temperature programmed techniques (reduction, oxidation, desorption)
CO-Chemisorption, NH₃-Chemisorption, CO₂-Chemisorption
FTIR with DRIFT cell

Gallery Catalyst Characterisation

Textural analysis (BET surface area, pore size and volume)

2 devices for TPR/TPO/TPD analysis and chemisorption

Catalytic Reactors

different glass stirred-tank reactors (10 – 5000 mL) for batch or continuous-flow processes
5 stainless steel pressure autoclaves (500 – 1500 mL) as stirred-tank reactor till 10 bar
2 glass stirred-tank reactors (180 and 300 mL) till 10 bar
5 high pressure and high temperature autoclaves made of stainless steel or hastelloy C (180, 300, 1000 mL) for temperatures till 350 °C and pressures till 150 bar
continuous-flow trickle-bed reactor with loop (temperature till 120 °C, pressure till 30 bar)
continuous-flow gas phase fixed-bed reactor (temperature till 750 °C, pressure till 100 bar)

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Institute of

AT Agricultural Technology